{"title":"Microwave Sintering","description":"\u003cp\u003e\u003cstrong\u003eMicrowave sintering densifies oxide and polyanion electrode powders in minutes rather than hours, with volumetric heating that suppresses grain coarsening and preserves the fine primary-particle morphology that lithium and sodium chemistries depend on.\u003c\/strong\u003e Energy couples directly into the susceptor or into the powder itself, so heat builds inside the compact instead of soaking inward from the furnace wall. For battery and solid-electrolyte researchers this means tighter control of cation ordering, less lithium loss, and a faster turnaround between formulation tweaks.\u003c\/p\u003e\n\n\u003cp\u003eMicrowave sintering is most useful for materials whose performance is set by how the final firing step is run:\u003c\/p\u003e\n\u003cul\u003e\n\u003cli\u003e\n\u003cstrong\u003eLayered oxide cathodes\u003c\/strong\u003e — NCM, NCA, and Li-rich layered systems, where short dwell times help retain Li\/Ni ordering and limit cation mixing.\u003c\/li\u003e\n\u003cli\u003e\n\u003cstrong\u003eOlivine and NASICON cathodes\u003c\/strong\u003e — LFP, LMFP, LVP, NVP, NVPF and related polyanion frameworks, which benefit from rapid carbon-coating pyrolysis and dense, conductive secondary particles.\u003c\/li\u003e\n\u003cli\u003e\n\u003cstrong\u003eSpinel cathodes\u003c\/strong\u003e — LMO and high-voltage LNMO, where minimizing Mn evaporation and preserving the cubic spinel ordering is critical.\u003c\/li\u003e\n\u003cli\u003e\n\u003cstrong\u003eAnode oxides\u003c\/strong\u003e — Li4Ti5O12 and Nb-based Wadsley-Roth phases, where fine grains and clean surfaces drive rate capability.\u003c\/li\u003e\n\u003cli\u003e\n\u003cstrong\u003eSolid electrolytes\u003c\/strong\u003e — garnet (LLZO), NASICON (LATP, LAGP), and perovskite (LLTO) ceramics, where high relative density and clean grain boundaries determine ionic conductivity.\u003c\/li\u003e\n\u003cli\u003e\n\u003cstrong\u003eCatalyst and fuel-cell supports\u003c\/strong\u003e — perovskite and fluorite oxides for SOFC cathodes and oxygen-evolution work, where rapid firing limits unwanted phase segregation.\u003c\/li\u003e\n\u003c\/ul\u003e\n\n\u003cp\u003eCompared with conventional box or tube furnaces, microwave systems trade some thermal uniformity for speed and energy efficiency, so most workflows pair a SiC or graphite susceptor crucible with a controlled atmosphere or sealed crucible. Pellet pressing, atmosphere control, and post-firing annealing remain the same as in conventional routes — the microwave step replaces only the long high-temperature dwell.\u003c\/p\u003e\n\n\u003cp\u003eIf you are screening cathode formulations and want shorter iteration cycles, start here; for slower, larger-batch firings under tightly controlled atmospheres, see Tube Furnaces and Box Furnaces. For upstream powder preparation, see \u003ca href=\"\/collections\/solid-state-synthesis\"\u003eSolid-State Synthesis\u003c\/a\u003e.\u003c\/p\u003e\n","products":[{"product_id":"enrsmmf","title":"ECS-N Mini Microwave Furnace (Max. 1550℃) for Rapid Sintering, ENRSMMF","description":"\u003cp\u003eA Mini Microwave Sintering Furnace is a high-speed, volumetric heating system designed for the rapid synthesis and densification of ceramic and battery materials. Unlike conventional muffle furnaces that heat from the outside-in via radiation, microwave furnaces heat the material itself from the inside-out, often reducing sintering times by 60% to 90%.\u003c\/p\u003e\n\u003cp\u003eFor microwave sintering, microwaves penetrate the material, causing molecular rotation (in dipoles) or ionic conduction. This generates heat volumetrically, ensuring the core and surface reach the target temperature almost simultaneously.\u003c\/p\u003e\n\u003ctable width=\"100%\"\u003e\n\u003ctbody\u003e\n\u003ctr\u003e\n\u003ctd\u003e\u003cem\u003ePart Number\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd\u003e\n\u003cul\u003e\n\u003cli\u003eENRSMMF (EN-RS-MMF)\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd\u003e\u003cem\u003eGeneral Features\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd\u003e\n\u003cul\u003e\n\u003cli\u003eThe microwave is directly applied on treated samples, which provides the heating rate is much faster than the conventional muffle furnace.\u003c\/li\u003e\n\u003cli\u003eThe energy consumption is 30%-60% less than the conventional resistance furnace. \u003c\/li\u003e\n\u003cli\u003eThe heating distribution around samples are uniform that makes the sintering samples have higher density and homogeneity. \u003c\/li\u003e\n\u003cli\u003eAccurate temperature control and measurement. \u003c\/li\u003e\n\u003cli\u003eMultiple gas types can be applied for various experiments\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd\u003e\u003cem\u003eMicrowave Furnace Features\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd\u003e\n\u003cul\u003e\n\u003cli\u003ePower: AC220V±10%, single-phases, 50\/60Hz, 1000 W\u003c\/li\u003e\n\u003cli\u003eHeating Element: Magnetron tube\u003c\/li\u003e\n\u003cli\u003eHeating Temperature: Max. 1550 ℃\u003c\/li\u003e\n\u003cli\u003eContinuous Operation Temperature: 1530 ℃\u003c\/li\u003e\n\u003cli\u003eRecommended Heating Rate: ≤10 ℃\/min\u003c\/li\u003e\n\u003cli\u003eFurnace Hearth: L120 * D120 * H60 mm\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd\u003e\u003cem\u003eHeating Experimental Data\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd\u003e\n\u003cul\u003e\n\u003cli\u003e0-1000 ℃, ~21 ℃\/min\u003c\/li\u003e\n\u003cli\u003e1000-1200 ℃, ~10 ℃\/min\u003c\/li\u003e\n\u003cli\u003e1200-1400 ℃, ~6 ℃\/min\u003c\/li\u003e\n\u003cli\u003e1400-1530 ℃, ~3 ℃\/min\u003c\/li\u003e\n\u003cli\u003eThermocouple: S-type, φ8*130mm\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd\u003e\u003cem\u003eNotes\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd\u003e\n\u003cul\u003e\n\u003cli\u003eThe door is not allowed to be opened when the furnace temperature higher than 300 ℃\u003c\/li\u003e\n\u003cli\u003eThe small crack appears on the furnace hearth is normal that won't affect the operation. \u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd\u003e\u003cem\u003eCertification\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd\u003e\n\u003cdiv\u003e\n\u003cul\u003e\n\u003cli\u003eCE certified\u003c\/li\u003e\n\u003cli\u003eUL and CSA certification is available upon request at extra cost\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/div\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd\u003e\u003cem\u003eDimension\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd\u003e\n\u003cdiv\u003e\n\u003cul\u003e\n\u003cli\u003eL514 × D480 × H720 mm\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/div\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd\u003e\u003cem\u003eWeight\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd\u003e\n\u003cdiv\u003e\n\u003cul\u003e\n\u003cli\u003e~40 kg\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/div\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003c\/tbody\u003e\n\u003c\/table\u003e\n\u003cp\u003e\u003cstrong\u003eReferences\u003c\/strong\u003e:\u003c\/p\u003e\n\u003cp\u003e\u003ca href=\"https:\/\/www.sciencedirect.com\/science\/article\/abs\/pii\/S037877531630814X\"\u003eJ. Wu, et al., Microwave sintering and in-situ transmission electron microscopy heating study of Li1·2(Mn0·53Co0.27)O2 with improved electrochemical performance, Journal of Power Sources, 2016, 326, 104-111\u003c\/a\u003e.\u003c\/p\u003e\n\u003cp\u003e\u003ca href=\"https:\/\/www.sciencedirect.com\/science\/article\/abs\/pii\/S0378775320312258\"\u003eX. Wang, et al., Low temperature and rapid microwave sintering of Na3Zr2Si2PO12 solid electrolytes for Na-Ion batteries, Journal of Power Sources, 2021, 481, 228924\u003c\/a\u003e\u003c\/p\u003e\n\u003cp\u003e\u003ca href=\"https:\/\/ceramics.onlinelibrary.wiley.com\/doi\/abs\/10.1111\/jace.12278\"\u003eK. I. Rybakov, et al., Microwave Sintering: Fundamentals and Modeling, J. Am. Ceramic Soc., 2013, 96, 1003-1020\u003c\/a\u003e.\u003cspan style=\"font-size: 0.875rem;\"\u003e \u003c\/span\u003e\u003c\/p\u003e","brand":"NBD","offers":[{"title":"Default Title","offer_id":47623122649318,"sku":"ENRSMMF","price":8888888.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0774\/6591\/1526\/files\/ENRSMMF_main.png?v=1777780142"},{"product_id":"enrsmfrs","title":"ECS-N Microwave Furnace (Max. 1600℃) with Rotary Stage for Rapid Sintering, ENRSMFRS","description":"\u003cp\u003eA Microwave Furnace with a Rotary Stage is a specialized high-temperature system that combines volumetric microwave heating with mechanical rotation. While standard microwave furnaces provide \"inside-out\" heating, they can occasionally suffer from \"hot spots\" due to the standing wave patterns within the microwave cavity. The addition of a rotary stage (rotating platform) ensures that the sample—whether a pellet or a powder—passes through multiple nodes of the electromagnetic field, resulting in the most uniform temperature distribution possible for Sodium-Ion (SIB) and Advanced Ceramic materials.\u003c\/p\u003e\n\u003cp\u003eIn a microwave cavity, the electric field intensity is not uniform. If a sample remains static, one side may reach 1550℃ while the other stays at 1400℃, leading to localized melting or non-uniform grain growth. (1) \u003cstrong\u003eField Averaging\u003c\/strong\u003e: By rotating the sample (typically 1–10 RPM), the furnace averages out the peaks and valleys of the microwave energy. (2) \u003cstrong\u003eUniform Densification\u003c\/strong\u003e: This is critical for Solid Electrolytes (like NASICON), where even minor temperature gradients can cause cracks or variations in ionic conductivity. (3) \u003cstrong\u003eBatch Consistency\u003c\/strong\u003e: If you are sintering multiple small pellets simultaneously, the rotary stage ensures every pellet experience the exact same thermal history.\u003c\/p\u003e\n\u003ctable width=\"100%\"\u003e\n\u003ctbody\u003e\n\u003ctr\u003e\n\u003ctd\u003e\u003cem\u003ePart Number\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd\u003e\n\u003cul\u003e\n\u003cli\u003eENRSMFRS (EN-RS-MFRS)\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd\u003e\u003cem\u003eGeneral Features\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd\u003e\n\u003cul\u003e\n\u003cli\u003eThe rotary stage is good for sample to be uniformly heated \u003c\/li\u003e\n\u003cli\u003eThe reliable design of microwave shield chamber \u003c\/li\u003e\n\u003cli\u003eThe microwave source is industrial grade with continuous adjustment. \u003c\/li\u003e\n\u003cli\u003eHMI touch screen control system for easy use\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd\u003e\u003cem\u003eMicrowave Furnace Features\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd\u003e\n\u003cul\u003e\n\u003cli\u003ePower: AC220V±10%, single-phases, 50\/60Hz, 3000 W\u003c\/li\u003e\n\u003cli\u003eHeating Element: Magnetron tube, output power: 0.2-1.4 kW, adjustable; output frequency: 2.45 GHz±25MHz\u003c\/li\u003e\n\u003cli\u003eWater cooling for heat dissipation\u003c\/li\u003e\n\u003cli\u003eHeating Temperature: Max. 1600 ℃\u003c\/li\u003e\n\u003cli\u003eThermocouple: IR type with temperature range of 300-1800℃\u003c\/li\u003e\n\u003cli\u003eStage Rotation Speed: \u003cspan style=\"color: rgb(255, 42, 0);\"\u003eMax. 5 r\/min\u003c\/span\u003e\n\u003c\/li\u003e\n\u003cli\u003eFurnace Hearth: L150 * D110 * H70 mm\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003cp\u003e         \u003cimg src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0774\/6591\/1526\/files\/ENRSMFRS_02_160x160.gif?v=1777783178\" style=\"margin-bottom: 16px; float: none;\"\u003e\u003c\/p\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd\u003e\u003cem\u003eNotes\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd\u003e\n\u003cul\u003e\n\u003cli\u003eBefore microwave furnace operation, please ensure the water chiller is turned on and function well. \u003c\/li\u003e\n\u003cli\u003eThe circulation water: hardness\u0026lt;10, inlet temperature: 5-30℃, outlet temperature: \u0026lt;50℃, water pressure: 0.06-0.12 MPa\u003c\/li\u003e\n\u003cli\u003eFrequently clean the dust, deposit, and other wasters inside the microwave chamber, which will cause high frequency arc to damage the microwave source. \u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd\u003e\u003cem\u003eCertification\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd\u003e\n\u003cdiv\u003e\n\u003cul\u003e\n\u003cli\u003eCE certified\u003c\/li\u003e\n\u003cli\u003eUL and CSA certification is available upon request at extra cost\u003c\/li\u003e\n\u003cli\u003eOne-year warranty and life-time technical support. \u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/div\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd\u003e\u003cem\u003eDimension\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd\u003e\n\u003cdiv\u003e\n\u003cul\u003e\n\u003cli\u003eL750 × D660× H600 mm\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/div\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd\u003e\u003cem\u003eWeight\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd\u003e\n\u003cdiv\u003e\n\u003cul\u003e\n\u003cli\u003e~50 kg\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/div\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003c\/tbody\u003e\n\u003c\/table\u003e\n\u003cp\u003e\u003cstrong\u003eReferences\u003c\/strong\u003e:\u003c\/p\u003e\n\u003cp\u003e\u003ca href=\"https:\/\/www.sciencedirect.com\/science\/article\/abs\/pii\/S037877531630814X\"\u003eJ. Wu, et al., Microwave sintering and in-situ transmission electron microscopy heating study of Li1·2(Mn0·53Co0.27)O2 with improved electrochemical performance, Journal of Power Sources, 2016, 326, 104-111\u003c\/a\u003e.\u003c\/p\u003e\n\u003cp\u003e\u003ca href=\"https:\/\/www.sciencedirect.com\/science\/article\/abs\/pii\/S0378775320312258\"\u003eX. Wang, et al., Low temperature and rapid microwave sintering of Na3Zr2Si2PO12 solid electrolytes for Na-Ion batteries, Journal of Power Sources, 2021, 481, 228924\u003c\/a\u003e\u003c\/p\u003e\n\u003cp\u003e\u003ca href=\"https:\/\/ceramics.onlinelibrary.wiley.com\/doi\/abs\/10.1111\/jace.12278\"\u003eK. I. Rybakov, et al., Microwave Sintering: Fundamentals and Modeling, J. Am. Ceramic Soc., 2013, 96, 1003-1020\u003c\/a\u003e.\u003cspan style=\"font-size: 0.875rem;\"\u003e \u003c\/span\u003e\u003c\/p\u003e","brand":"NBD","offers":[{"title":"Default Title","offer_id":47623167967462,"sku":"ENRSMFRS","price":8888888.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0774\/6591\/1526\/files\/ENRSMFRS_main.png?v=1777782758"},{"product_id":"emhmmtf","title":"ECS-M Hybrid Microwave Muffle\/Tube Furnace (1000°C), EMHMMTF","description":"\u003cp\u003eA Hybrid Microwave Muffle\/Tube Furnace (1000°C) is a cutting-edge thermal processing system that integrates conventional resistance heating (coils) with microwave energy. It overcomes the \"Transparency\" problem of microwaves at low temperatures by using resistance coils to pre-heat materials until they become microwave-absorbent, at which point microwave energy provides ultra-fast, volumetric heating to the core.\u003c\/p\u003e\n\u003cp\u003eTraditional microwave-only furnaces often struggle with materials that have low dielectric loss at room temperature. The Hybrid system solves this through a dual-action mechanism: (1) \u003cstrong\u003eResistance Heating (Surface-In)\u003c\/strong\u003e: Provides stable, uniform background heating to the chamber. It acts as the \"starter\" to bring the sample to its \"coupling temperature.\" (2) \u003cstrong\u003eMicrowave Heating (Core-Out)\u003c\/strong\u003e: Once the material begins to absorb microwaves, energy is delivered directly to the molecular level. This results in \"Inverse Temperature Gradients,\" where the core of the sample can be slightly hotter than the surface, promoting perfect densification.\u003c\/p\u003e\n\u003ctable width=\"100%\" style=\"height: 201.2px;\"\u003e\n\u003ctbody\u003e\n\u003ctr style=\"height: 35.6px;\"\u003e\n\u003ctd style=\"width: 17.9856%; height: 35.6px;\"\u003e\u003cem\u003ePart Number\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd style=\"width: 81.6547%; height: 35.6px;\"\u003e\n\u003cul\u003e\n\u003cli\u003eEMHTMR (EM-HTMR)\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd style=\"width: 17.9856%;\"\u003e\u003cem\u003ePower\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd style=\"width: 81.6547%;\"\u003e\n\u003cul\u003e\n\u003cli\u003eAC220V±10%, single-phase, 50\/60Hz, 1300W\u003cbr\u003e\n\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr style=\"height: 35.6px;\"\u003e\n\u003ctd style=\"width: 17.9856%; height: 35.6px;\"\u003e\u003cem\u003eKey Features for Hybrid Microwave Furnace\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd style=\"width: 81.6547%; height: 35.6px;\"\u003e\n\u003cul\u003e\n\u003cli\u003eMicrowave Source Power: 800W, 2450 MHz, continuous power output (no pulse)\u003c\/li\u003e\n\u003cli\u003eReactor Material: SS304, inside coated with PTFE for anti-corrosion purpose\u003c\/li\u003e\n\u003cli\u003eInside Chamber Volume: ~1.2 L\u003c\/li\u003e\n\u003cli\u003eHigh Temperature \u003cspan style=\"color: rgb(255, 42, 0);\"\u003eMuffle Furnace\u003c\/span\u003e: 100*100 mm Al2O3 crucible. Other material types, such as ZrO2, BN, Graphite, can be supplied upon request.\u003c\/li\u003e\n\u003cli\u003eHigh Temperature \u003cspan style=\"color: rgb(255, 42, 0);\"\u003eTube Furnace\u003c\/span\u003e: Φ40mm quartz tube inserted from the top side and the T-shape gas flow system inside for solid-gas reaction. \u003c\/li\u003e\n\u003cli\u003eDesign Temperature: \u003cspan style=\"color: rgb(255, 42, 0);\"\u003e0-1000°C. \u003cspan style=\"color: rgb(0, 0, 0);\"\u003eThermocouple for temperature measurement.\u003c\/span\u003e\u003c\/span\u003e\n\u003c\/li\u003e\n\u003cli\u003ePLC control and HMI touch screen monitor\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd style=\"width: 17.9856%;\"\u003e\u003cem\u003eCertification\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd style=\"width: 81.6547%;\"\u003e\n\u003cdiv style=\"text-align: left;\"\u003e\n\u003cul\u003e\n\u003cli\u003eCE certified\u003c\/li\u003e\n\u003cli\u003eUL and CSA certification is available upon request at extra cost\u003c\/li\u003e\n\u003cli\u003eOne-year warranty and life-time technical support.\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/div\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd style=\"width: 17.9856%;\"\u003e\u003cem\u003eDimension\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd style=\"width: 81.6547%;\"\u003e\n\u003cdiv style=\"text-align: left;\"\u003e\n\u003cul\u003e\n\u003cli\u003eL620 * W490 * H620 mm\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/div\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd style=\"width: 17.9856%;\"\u003e\u003cem\u003eWeight\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd style=\"width: 81.6547%;\"\u003e\n\u003cdiv style=\"text-align: left;\"\u003e\n\u003cul\u003e\n\u003cli\u003e~50 kg\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/div\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003c\/tbody\u003e\n\u003c\/table\u003e\n\u003cp\u003e \u003c\/p\u003e\n\u003cp\u003e\u003cstrong\u003eReferences\u003c\/strong\u003e:\u003c\/p\u003e\n\u003cp\u003e\u003ca href=\"https:\/\/pubs.acs.org\/doi\/abs\/10.1021\/acsaem.5c03691\"\u003eG. Liu, et al., Heating-Rate Controlled Microwave Co-Pyrolysis for Synergistically Doped Carbon Electrode Materials, ACS Appl. Energy Mater. 2026, 9, 5, 2600–2610\u003c\/a\u003e\u003c\/p\u003e\n\u003cp\u003e\u003ca href=\"https:\/\/www.sciencedirect.com\/science\/article\/abs\/pii\/S0013468613005768\"\u003eP. Gao, et al., Microwave rapid preparation of LiNi0.5Mn1.5O4 and the improved high rate performance for lithium-ion batteries, Electrochimica Acta, 2013, 100, 125-132.\u003c\/a\u003e\u003c\/p\u003e","brand":"MKW","offers":[{"title":"Default Title","offer_id":47630203584742,"sku":"EMHMMTF","price":8888888.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0774\/6591\/1526\/files\/EMHMMTF_main.png?v=1777998319"},{"product_id":"emmfbf","title":"ECS-M Microwave Fluidized Bed Furnace (1200°C), EMMFBF","description":"\u003cp\u003eA Microwave Fluidized Bed Furnace (MW-FBF) is a high-efficiency reactor that integrates the rapid, volumetric heating of microwaves with the superior mass and heat transfer of a fluidized bed. The MW-FBF heats the particles directly (inside-out), allowing the gas to stay cooler and act purely as a fluidizing and protective medium.\u003c\/p\u003e\n\u003cp\u003eThis hybrid system solves the \"hot spot\" problem found in static microwave synthesis and the \"thermal lag\" of conventional gas-heated fluidized beds. (1) \u003cstrong\u003eMicrowave Interaction\u003c\/strong\u003e: The microwave energy penetrates the reactor wall (usually made of microwave-transparent Quartz or Alumina) and couples directly with the battery powders (e.g., NFPP or Carbon-coated NNFMO). (2) \u003cstrong\u003eFluidization State\u003c\/strong\u003e: The upward gas flow keeps the particles in a \"boiling\" state. This constant, chaotic motion ensures that every particle is exposed to the microwave field for the exact same amount of time. (3) \u003cstrong\u003eVolumetric Uniformity\u003c\/strong\u003e: Because the heat is generated within the moving particles, temperature gradients across the bed are typically reduced to only a few Kelvin.\u003c\/p\u003e\n\u003ctable width=\"100%\" style=\"height: 201.2px;\"\u003e\n\u003ctbody\u003e\n\u003ctr style=\"height: 35.6px;\"\u003e\n\u003ctd style=\"width: 17.9856%; height: 35.6px;\"\u003e\u003cem\u003ePart Number\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd style=\"width: 81.6547%; height: 35.6px;\"\u003e\n\u003cul\u003e\n\u003cli\u003eEMMFBF (EM-MFBF)\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd style=\"width: 17.9856%;\"\u003e\u003cem\u003ePower\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd style=\"width: 81.6547%;\"\u003e\n\u003cul\u003e\n\u003cli\u003eAC380V±10%, three-phases, 50\/60Hz, 10 kW\u003cbr\u003e\n\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr style=\"height: 35.6px;\"\u003e\n\u003ctd style=\"width: 17.9856%; height: 35.6px;\"\u003e\u003cem\u003eKey Features for Microwave Fluidized Furnace\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd style=\"width: 81.6547%; height: 35.6px;\"\u003e\n\u003cul\u003e\n\u003cli\u003eMicrowave Source Power: 1600W, 2450 MHz, continuous power output (no pulse)\u003c\/li\u003e\n\u003cli\u003eThe system is composed of feeder, gas inlet, heating vessel, microwave setup, gas outlet, and control part. \u003c\/li\u003e\n\u003cli\u003eFeeder: SS304, two-stage screw feeding, water cooling jacket\u003c\/li\u003e\n\u003cli\u003eGas Inlet: quartz, gas flow from bottom and wrapped with insulation material for pre-heating\u003c\/li\u003e\n\u003cli\u003eHeating Vessel: quartz, 1200 °C. A high temperature gas flow plate is designed at the bottom\u003c\/li\u003e\n\u003cli\u003eMicrowave Setup: It is composed of microwave cavity, power source, anti-leaking door, and insulation layer. \u003c\/li\u003e\n\u003cli\u003eGas Outlet: SS304, wrapped with insulation material for temperature maintenance. \u003cbr\u003e\n\u003c\/li\u003e\n\u003cli\u003ePLC control and HMI touch screen monitor for temperature, power, and other status. \u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd style=\"width: 17.9856%;\"\u003e\u003cem\u003eCertification\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd style=\"width: 81.6547%;\"\u003e\n\u003cdiv style=\"text-align: left;\"\u003e\n\u003cul\u003e\n\u003cli\u003eCE certified\u003c\/li\u003e\n\u003cli\u003eUL and CSA certification is available upon request at extra cost\u003c\/li\u003e\n\u003cli\u003eOne-year warranty and life-time technical support.\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/div\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd style=\"width: 17.9856%;\"\u003e\u003cem\u003eDimension\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd style=\"width: 81.6547%;\"\u003e\n\u003cdiv style=\"text-align: left;\"\u003e\n\u003cul\u003e\n\u003cli\u003eL2500 * W1500 * H1800 mm\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/div\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd style=\"width: 17.9856%;\"\u003e\u003cem\u003eWeight\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd style=\"width: 81.6547%;\"\u003e\n\u003cdiv style=\"text-align: left;\"\u003e\n\u003cul\u003e\n\u003cli\u003e~150 kg\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/div\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003c\/tbody\u003e\n\u003c\/table\u003e\n\u003cp\u003e \u003c\/p\u003e\n\u003cp\u003e\u003cstrong\u003eReferences\u003c\/strong\u003e:\u003c\/p\u003e\n\u003cp\u003e\u003ca href=\"https:\/\/scijournals.onlinelibrary.wiley.com\/doi\/abs\/10.1002\/bbb.1780\"\u003eM. Adam, et al., Microwave fluidized bed for biomass pyrolysis. Part I: Process design, Biofpr. 2017, 11, 601-612\u003c\/a\u003e\u003c\/p\u003e\n\u003cp\u003e\u003ca href=\"https:\/\/www.sciencedirect.com\/science\/article\/abs\/pii\/S1359431123010384\"\u003eY. Cui, et al., Microwave heating of silicon carbide and polypropylene particles in a fluidized bed reactor, Applied Thermal Engineering, 2023, 232, 121009\u003c\/a\u003e\u003c\/p\u003e","brand":"MKW","offers":[{"title":"Default Title","offer_id":47630415790310,"sku":"EMMFBF","price":8888888.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0774\/6591\/1526\/files\/EMMFBF_main.png?v=1778009955"},{"product_id":"emmhtf","title":"ECS-M Microwave Horizontal Tube Furnace (1200 or 1600°C, -99 KPa), EMMHTF","description":"\u003cp\u003eA Horizontal Microwave Tube Furnace is a precision thermal processing instrument that combines the atmospheric control of a tube furnace with the ultra-fast, volumetric heating of microwaves. Unlike a muffle furnace, the horizontal tube design allows for a continuous flow of inert gas (Ar, N2) or reactive gas (H2) across your sample, which is critical for protecting sensitive sodium and iron species from oxidation.\u003c\/p\u003e\n\u003cp\u003eThe microwave tube furnace system typically consists of a high-purity Quartz or Alumina tube passing through a microwave cavity. (1) \u003cstrong\u003eAtmosphere Integrity\u003c\/strong\u003e: The horizontal orientation makes it easy to seal the tube ends with water-cooled vacuum flanges. This allows you to perform vacuum sintering or process materials in a high-purity reducing atmosphere (Ar+5% H2). (2) \u003cstrong\u003eVolumetric Uniformity\u003c\/strong\u003e: Microwaves heat the sample from the \"inside-out.\" In a horizontal tube, the microwave field is optimized to provide a uniform hot zone in the center, ensuring pellets or powders are heated evenly throughout their entire cross-section. (3) \u003cstrong\u003eThermal Shock Resistance\u003c\/strong\u003e: Alumina tubes are specially engineered to withstand the rapid ramp rates (up to 100 °C\/min) that microwave heating provides.\u003c\/p\u003e\n\u003ctable style=\"height: 201.2px;\" width=\"100%\"\u003e\n\u003ctbody\u003e\n\u003ctr style=\"height: 35.6px;\"\u003e\n\u003ctd style=\"width: 17.9856%; height: 35.6px;\"\u003e\u003cem\u003ePart Number\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd style=\"width: 81.6547%; height: 35.6px;\"\u003e\n\u003cul\u003e\n\u003cli\u003eEMMHTF (EM-MHTF)\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd style=\"width: 17.9856%;\"\u003e\u003cem\u003ePower\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd style=\"width: 81.6547%;\"\u003e\n\u003cul\u003e\n\u003cli\u003eAC220V±10%, single-phase, 50\/60Hz, 3000W for 1200°C version\u003cbr\u003e\n\u003c\/li\u003e\n\u003cli\u003eAC380V±10%, three-phases, 50\/60Hz, 5500W for 1600°C version\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr style=\"height: 35.6px;\"\u003e\n\u003ctd style=\"width: 17.9856%; height: 35.6px;\"\u003e\u003cem\u003eKey Features for Microwave tube Furnace\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd style=\"width: 81.6547%; height: 35.6px;\"\u003e\n\u003cul\u003e\n\u003cli\u003eMicrowave Source Power: 1600W (1200°C) or 3200 W (1600°C), 2450 MHz, continuous power output (no pulse)\u003c\/li\u003e\n\u003cli\u003eReactor Material: SS304 with high sealing quality and good heating insulation. \u003cbr\u003e\n\u003c\/li\u003e\n\u003cli\u003eHigh Temperature \u003cspan style=\"color: rgb(0, 0, 0);\"\u003eTube Furnace\u003c\/span\u003e: Φ50mm (1200°C) or Φ100mm (1600°C) quartz tube is horizontally placed in the furnace hearth\u003c\/li\u003e\n\u003cli\u003eA 20 mL (1200°C) or 100 mL (1600°C) quartz crucible boat is included. Other material types, such as alumina, BN, hastelloy, and graphite can be supplied upon request. \u003c\/li\u003e\n\u003cli\u003eDesign Temperature: (1) Max. \u003cspan style=\"color: rgb(255, 42, 0);\"\u003e1200°C. \u003cspan style=\"color: rgb(0, 0, 0);\"\u003eThe continuous operation temperature is 1100 °C (±1℃). (2) Max. \u003cspan style=\"color: rgb(255, 42, 0);\"\u003e1600°C. \u003cspan style=\"color: rgb(0, 0, 0);\"\u003eThe continuous operation temperature is 1500 °C (±1℃).\u003c\/span\u003e\u003c\/span\u003e Thermocouple is used for temperature measurement. \u003c\/span\u003e\u003c\/span\u003e\n\u003c\/li\u003e\n\u003cli\u003e\u003cspan style=\"color: rgb(255, 42, 0);\"\u003e\u003cspan style=\"color: rgb(0, 0, 0);\"\u003eThe two-channels gas inlet and outlet are included.\u003c\/span\u003e\u003c\/span\u003e\u003c\/li\u003e\n\u003cli\u003e\u003cspan style=\"color: rgb(255, 42, 0);\"\u003e\u003cspan style=\"color: rgb(0, 0, 0);\"\u003eVacuum Operation: down to -0.099 MPa. The vacuum pump (eg: \u003ca href=\"https:\/\/echemsupplies.com\/products\/edsrvvp?variant=47513025282278\"\u003eEDSRVVP\u003c\/a\u003e) is not included and can be additionally purchased.  \u003c\/span\u003e\u003c\/span\u003e\u003c\/li\u003e\n\u003cli\u003ePLC control and HMI touch screen monitor\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd style=\"width: 17.9856%;\"\u003e\u003cem\u003eCertification\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd style=\"width: 81.6547%;\"\u003e\n\u003cdiv style=\"text-align: left;\"\u003e\n\u003cul\u003e\n\u003cli\u003eCE certified\u003c\/li\u003e\n\u003cli\u003eUL and CSA certification is available upon request at extra cost\u003c\/li\u003e\n\u003cli\u003eOne-year warranty and life-time technical support.\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/div\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd style=\"width: 17.9856%;\"\u003e\u003cem\u003eDimension\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd style=\"width: 81.6547%;\"\u003e\n\u003cdiv style=\"text-align: left;\"\u003e\n\u003cul\u003e\n\u003cli\u003eL1500 * W650 * H800 mm\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/div\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd style=\"width: 17.9856%;\"\u003e\u003cem\u003eWeight\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd style=\"width: 81.6547%;\"\u003e\n\u003cdiv style=\"text-align: left;\"\u003e\n\u003cul\u003e\n\u003cli\u003e~75 kg\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/div\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003c\/tbody\u003e\n\u003c\/table\u003e\n\u003cp\u003e \u003c\/p\u003e\n\u003cp\u003e\u003cstrong\u003eReferences\u003c\/strong\u003e:\u003c\/p\u003e\n\u003cp\u003e\u003ca href=\"https:\/\/pubs.acs.org\/doi\/abs\/10.1021\/acsaem.5c03691\"\u003eG. Liu, et al., Heating-Rate Controlled Microwave Co-Pyrolysis for Synergistically Doped Carbon Electrode Materials, ACS Appl. Energy Mater. 2026, 9, 5, 2600–2610\u003c\/a\u003e\u003c\/p\u003e\n\u003cp\u003e\u003ca href=\"https:\/\/www.sciencedirect.com\/science\/article\/abs\/pii\/S0013468613005768\"\u003eP. Gao, et al., Microwave rapid preparation of LiNi0.5Mn1.5O4 and the improved high rate performance for lithium-ion batteries, Electrochimica Acta, 2013, 100, 125-132.\u003c\/a\u003e\u003c\/p\u003e","brand":"MKW","offers":[{"title":"1200°C","offer_id":47631381168358,"sku":"EMMHTF1200","price":8888888.0,"currency_code":"USD","in_stock":true},{"title":"1600°C","offer_id":47631381201126,"sku":"EMMHTF1600","price":8888888.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0774\/6591\/1526\/files\/EMMHTF_main.png?v=1778048246"},{"product_id":"emmvmf","title":"ECS-M Microwave Vacuum Muffle Furnace (1400°C, -99 KPa), EMMVMF","description":"\u003cp\u003eA Microwave Vacuum Muffle Furnace is a high-performance thermal processing system that integrates volumetric microwave heating with a sealed vacuum chamber. By combining the \"inside-out\" heating speed of microwaves with the oxygen-free environment of a high vacuum, it enables rapid densification and phase-pure synthesis that conventional muffle furnaces cannot match.\u003c\/p\u003e\n\u003cp\u003eThis hybrid configuration solves the two greatest challenges in battery powder synthesis: Slow Thermal Diffusion and Oxidation. (1) \u003cstrong\u003eVolumetric Heating (Microwave)\u003c\/strong\u003e: Standard vacuum furnaces rely on radiation, which is slow in a vacuum because there is no air to conduct heat. Microwaves bypass this by coupling directly with the material's dipoles, generating heat internally and allowing for ramp rates exceeding 50°C\/min. (2) \u003cstrong\u003eContamination-Free Environment (Vacuum)\u003c\/strong\u003e: Removing air prevents the oxidation of transition metals (like Fe2+ in NFPP). \u003c\/p\u003e\n\u003ctable width=\"100%\" style=\"height: 201.2px;\"\u003e\n\u003ctbody\u003e\n\u003ctr style=\"height: 35.6px;\"\u003e\n\u003ctd style=\"width: 17.9856%; height: 35.6px;\"\u003e\u003cem\u003ePart Number\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd style=\"width: 81.6547%; height: 35.6px;\"\u003e\n\u003cul\u003e\n\u003cli\u003eEMMVMF (EM-MVMF)\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd style=\"width: 17.9856%;\"\u003e\u003cem\u003ePower\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd style=\"width: 81.6547%;\"\u003e\n\u003cul\u003e\n\u003cli\u003eAC220V±10%, single-phase, 50\/60Hz, 3500W\u003cbr\u003e\n\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr style=\"height: 35.6px;\"\u003e\n\u003ctd style=\"width: 17.9856%; height: 35.6px;\"\u003e\u003cem\u003eKey Features for Microwave tube Furnace\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd style=\"width: 81.6547%; height: 35.6px;\"\u003e\n\u003cul\u003e\n\u003cli\u003eMicrowave Source Power: 1600W, 2450 MHz, continuous power output (no pulse)\u003c\/li\u003e\n\u003cli\u003eReactor Material: SS304 with high sealing quality and good heating insulation. \u003cbr\u003e\n\u003c\/li\u003e\n\u003cli\u003eHigh Temperature \u003cspan style=\"color: rgb(0, 0, 0);\"\u003eSystem\u003c\/span\u003e: 100*100mm alumina crucible. Other material types, such as alumina, BN, hastelloy, and graphite can be supplied upon request. \u003c\/li\u003e\n\u003cli\u003eDesign Temperature: Max. \u003cspan style=\"color: rgb(255, 42, 0);\"\u003e1400°C (continuous operation at1300°C, \u003cspan style=\"color: rgb(0, 0, 0);\"\u003e\u003cspan style=\"color: rgb(255, 42, 0);\"\u003e±1℃\u003c\/span\u003e). Non-contact IR temperature measurement is used. \u003c\/span\u003e\u003c\/span\u003e\n\u003c\/li\u003e\n\u003cli\u003e\u003cspan style=\"color: rgb(255, 42, 0);\"\u003e\u003cspan style=\"color: rgb(0, 0, 0);\"\u003eThe two-channels gas inlet and outlet are included. More channels version can be supplied upon request.  \u003c\/span\u003e\u003c\/span\u003e\u003c\/li\u003e\n\u003cli\u003e\u003cspan style=\"color: rgb(255, 42, 0);\"\u003e\u003cspan style=\"color: rgb(0, 0, 0);\"\u003eVacuum Operation: down to -99 KPa. The vacuum pump (eg: \u003ca href=\"https:\/\/echemsupplies.com\/products\/edsrvvp?variant=47513025282278\"\u003eEDSRVVP\u003c\/a\u003e) is not included and can be additionally purchased.  \u003c\/span\u003e\u003c\/span\u003e\u003c\/li\u003e\n\u003cli\u003ePLC control and HMI touch screen monitor\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd style=\"width: 17.9856%;\"\u003e\u003cem\u003eCertification\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd style=\"width: 81.6547%;\"\u003e\n\u003cdiv style=\"text-align: left;\"\u003e\n\u003cul\u003e\n\u003cli\u003eCE certified\u003c\/li\u003e\n\u003cli\u003eUL and CSA certification is available upon request at extra cost\u003c\/li\u003e\n\u003cli\u003eOne-year warranty and life-time technical support.\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/div\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd style=\"width: 17.9856%;\"\u003e\u003cem\u003eDimension\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd style=\"width: 81.6547%;\"\u003e\n\u003cdiv style=\"text-align: left;\"\u003e\n\u003cul\u003e\n\u003cli\u003eL700 * W600 * H800 mm\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/div\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd style=\"width: 17.9856%;\"\u003e\u003cem\u003eWeight\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd style=\"width: 81.6547%;\"\u003e\n\u003cdiv style=\"text-align: left;\"\u003e\n\u003cul\u003e\n\u003cli\u003e~80 kg\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/div\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003c\/tbody\u003e\n\u003c\/table\u003e\n\u003cp\u003e \u003c\/p\u003e\n\u003cp\u003e\u003cstrong\u003eReferences\u003c\/strong\u003e:\u003c\/p\u003e\n\u003cp\u003e\u003ca href=\"https:\/\/pubs.acs.org\/doi\/abs\/10.1021\/acsaem.5c03691\"\u003eG. Liu, et al., Heating-Rate Controlled Microwave Co-Pyrolysis for Synergistically Doped Carbon Electrode Materials, ACS Appl. Energy Mater. 2026, 9, 5, 2600–2610\u003c\/a\u003e\u003c\/p\u003e\n\u003cp\u003e\u003ca href=\"https:\/\/www.sciencedirect.com\/science\/article\/abs\/pii\/S0013468613005768\"\u003eP. Gao, et al., Microwave rapid preparation of LiNi0.5Mn1.5O4 and the improved high rate performance for lithium-ion batteries, Electrochimica Acta, 2013, 100, 125-132.\u003c\/a\u003e\u003c\/p\u003e","brand":"MKW","offers":[{"title":"Default Title","offer_id":47631102116070,"sku":"EMMVMF","price":8888888.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0774\/6591\/1526\/files\/EMMVMF_main.png?v=1778038440"},{"product_id":"emhmmvtf","title":"ECS-M Hybrid Microwave Muffle \u0026 Vertical Tube Furnace (1200°C, -99 KPa), EMHMMVTF","description":"\u003cp\u003eA Microwave Vertical Tube Furnace is a high-precision thermal processing system that combines the rapid, volumetric heating of microwaves with the inherent temperature uniformity of a vertical orientation. The vertical design leverages natural convection to create a highly stable thermal environment, which, when coupled with microwave energy, allows for \"flash\" reactions that are nearly impossible in traditional resistive furnaces.\u003c\/p\u003e\n\u003cp\u003eThe vertical orientation (often called a \"Top-Loading\" or \"Fall-Through\" configuration) offers several unique benefits: (1) \u003cstrong\u003eNatural Convection\u003c\/strong\u003e: Heated gases naturally rise, creating a continuous convective loop inside the tube. This actively mixes the atmosphere, smoothing out hot spots and resulting in superior axial temperature uniformity compared to horizontal designs. (2) \u003cstrong\u003eContamination Control\u003c\/strong\u003e: In a vertical setup, gravity pulls microscopic particles generated during the reaction straight down, past the sample and away from critical surfaces. This is vital for semiconductor-grade battery coatings and high-purity battery material synthesis. (3) \u003cstrong\u003eSpace Efficiency\u003c\/strong\u003e: The vertical footprint is significantly smaller than a horizontal unit, making it ideal for crowded laboratories with limited space.  \u003c\/p\u003e\n\u003ctable style=\"height: 201.2px;\" width=\"100%\"\u003e\n\u003ctbody\u003e\n\u003ctr style=\"height: 35.6px;\"\u003e\n\u003ctd style=\"width: 17.9856%; height: 35.6px;\"\u003e\u003cem\u003ePart Number\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd style=\"width: 81.6547%; height: 35.6px;\"\u003e\n\u003cul\u003e\n\u003cli\u003eEMHMMVTF (EM-HMMVTF)\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd style=\"width: 17.9856%;\"\u003e\u003cem\u003ePower\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd style=\"width: 81.6547%;\"\u003e\n\u003cul\u003e\n\u003cli\u003eAC220V±10%, single-phase, 50\/60Hz, 2600W\u003cbr\u003e\n\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr style=\"height: 35.6px;\"\u003e\n\u003ctd style=\"width: 17.9856%; height: 35.6px;\"\u003e\u003cem\u003eKey Features for Microwave tube Furnace\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd style=\"width: 81.6547%; height: 35.6px;\"\u003e\n\u003cul\u003e\n\u003cli\u003ePLC control and HMI touch screen monitor\u003c\/li\u003e\n\u003cli\u003eMicrowave Source Power: 1600W, 2450 MHz, continuous power output (no pulse)\u003c\/li\u003e\n\u003cli\u003eReactor Material: SS304 with high sealing quality and good heating insulation.\u003c\/li\u003e\n\u003cli\u003eInner Chamber Size: 5 L, which suitable for both microwave muffle and inserted tube furnace application. \u003cbr\u003e\n\u003c\/li\u003e\n\u003cli\u003eMuffle Furnace Use: 100*100mm quartz or alumina crucible. \u003c\/li\u003e\n\u003cli\u003eOther material types, such as alumina, BN, hastelloy, and graphite can be supplied upon request. \u003c\/li\u003e\n\u003cli\u003eHigh Temperature \u003cspan style=\"color: rgb(255, 42, 0);\"\u003eTube Furnace\u003c\/span\u003e: Φ40mm quartz tube is vertically installed in the furnace hearth and F-shape side gas flow system is presented. \u003cbr\u003e\n\u003c\/li\u003e\n\u003cli\u003eDesign Temperature: \u003cspan style=\"color: rgb(255, 42, 0);\"\u003e\u003cspan style=\"color: rgb(0, 0, 0);\"\u003e0-1200°C.\u003c\/span\u003e \u003cspan style=\"color: rgb(0, 0, 0);\"\u003eThe continuous operation temperature is \u003cspan style=\"color: rgb(255, 42, 0);\"\u003e1100 °C (±1℃)\u003c\/span\u003e. Thermocouple is used for temperature measurement.\u003c\/span\u003e\u003c\/span\u003e\n\u003c\/li\u003e\n\u003cli\u003e\u003cspan style=\"color: rgb(255, 42, 0);\"\u003e\u003cspan style=\"color: rgb(0, 0, 0);\"\u003eThe two- or more channels gas flow control unit can be supplied upon request (\u003cstrong\u003enot included\u003c\/strong\u003e)\u003c\/span\u003e\u003c\/span\u003e\u003c\/li\u003e\n\u003cli\u003e\u003cspan style=\"color: rgb(255, 42, 0);\"\u003e\u003cspan style=\"color: rgb(0, 0, 0);\"\u003eOne channel is liquid feeding with pre-heating (300\u003cspan style=\"color: rgb(255, 42, 0);\"\u003e\u003cspan style=\"color: rgb(0, 0, 0);\"\u003e°C\u003c\/span\u003e\u003c\/span\u003e) for gas vaporization is available (\u003cstrong\u003enot included\u003c\/strong\u003e).  \u003c\/span\u003e\u003c\/span\u003e\u003c\/li\u003e\n\u003cli\u003e\n\u003cspan style=\"color: rgb(255, 42, 0);\"\u003e\u003cspan style=\"color: rgb(0, 0, 0);\"\u003eVacuum Operation: down to -0.099 MPa. The vacuum pump (eg: \u003ca href=\"https:\/\/echemsupplies.com\/products\/edsrvvp?variant=47513025282278\"\u003eEDSRVVP\u003c\/a\u003e) is not included and can be additionally purchased.  \u003c\/span\u003e\u003c\/span\u003e      \u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd style=\"width: 17.9856%;\"\u003e\u003cem\u003eCertification\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd style=\"width: 81.6547%;\"\u003e\n\u003cdiv style=\"text-align: left;\"\u003e\n\u003cul\u003e\n\u003cli\u003eCE certified\u003c\/li\u003e\n\u003cli\u003eUL and CSA certification is available upon request at extra cost\u003c\/li\u003e\n\u003cli\u003eOne-year warranty and life-time technical support.\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/div\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd style=\"width: 17.9856%;\"\u003e\u003cem\u003eDimension\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd style=\"width: 81.6547%;\"\u003e\n\u003cdiv style=\"text-align: left;\"\u003e\n\u003cul\u003e\n\u003cli\u003eL1500 * W650 * H800 mm\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/div\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd style=\"width: 17.9856%;\"\u003e\u003cem\u003eWeight\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd style=\"width: 81.6547%;\"\u003e\n\u003cdiv style=\"text-align: left;\"\u003e\n\u003cul\u003e\n\u003cli\u003e~75 kg\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/div\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003c\/tbody\u003e\n\u003c\/table\u003e\n\u003cp\u003e \u003c\/p\u003e\n\u003cp\u003e\u003cstrong\u003eReferences\u003c\/strong\u003e:\u003c\/p\u003e\n\u003cp\u003e\u003ca href=\"https:\/\/pubs.acs.org\/doi\/abs\/10.1021\/acsaem.5c03691\"\u003eG. Liu, et al., Heating-Rate Controlled Microwave Co-Pyrolysis for Synergistically Doped Carbon Electrode Materials, ACS Appl. Energy Mater. 2026, 9, 5, 2600–2610\u003c\/a\u003e\u003c\/p\u003e\n\u003cp\u003e\u003ca href=\"https:\/\/www.sciencedirect.com\/science\/article\/abs\/pii\/S0013468613005768\"\u003eP. Gao, et al., Microwave rapid preparation of LiNi0.5Mn1.5O4 and the improved high rate performance for lithium-ion batteries, Electrochimica Acta, 2013, 100, 125-132.\u003c\/a\u003e\u003c\/p\u003e","brand":"MKW","offers":[{"title":"Default Title","offer_id":47631263695078,"sku":"EMHMMVTF","price":8888888.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0774\/6591\/1526\/files\/EMHMMVTF_01.png?v=1778045886"}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0774\/6591\/1526\/collections\/ENRSMMF_main.png?v=1778030576","url":"https:\/\/echemsupplies.com\/collections\/microwave-sintering.oembed","provider":"EChem Supplies","version":"1.0","type":"link"}