{"product_id":"ekmbabrmss","title":"ECS-KM Benchtop Automatic Batch Reactor (Max. 10 MPa, 300°C, 1 L) with Mechanical Shaft Stirring, EKMBABRMSS","description":"\u003cp\u003eA benchtop automatic batch reactor with mechanical shaft stirring is the cornerstone equipment for process chemistry optimization, scale-up modeling, and precise kinetic control (e.g., polymerizations, slurry syntheses, crystallization, and controlled dosing reactions). Unlike simple magnetic stirrers, overhead mechanical shaft drives provide high torque to handle viscous reaction media, phase-transfer slurries, and precise, non-slip speed regulation across 50 to 2000 RPM.\u003c\/p\u003e\n\u003cp data-path-to-node=\"0\"\u003eThe benchtop automated reactors integrate real-time sensor feedback with programmable logic controllers (PLCs) or PC software: (1) \u003cstrong\u003eClosed-Loop Temperature Control\u003c\/strong\u003e: Cascaded PID loops monitor both internal bed\/reaction temperature and jacket fluid temperature, dynamically adjusting heating\/cooling circulators to handle fast exothermic or endothermic spikes. (2) \u003cstrong\u003eAutomated Dosing \u0026amp; Feed Controls\u003c\/strong\u003e: Synchronized syringe or peristaltic pumps deliver reagents based on elapsed time, pH thresholds, or maximum heat-flow dissipation limits (preventing thermal runaway). (3) \u003cstrong\u003eTorque \u0026amp; Viscosity Monitoring\u003c\/strong\u003e: Real-time feedback from the mechanical stirrer motor tracks shaft torque (N.cm), allowing continuous calculation of slurry viscosity changes or polymerization progress in situ. (4) \u003cstrong\u003eData Logging\u003c\/strong\u003e: Continuous recording of Treactor}, Tjacket, stirrer RPM, torque, system pressure, pH, and dosing rate for process analytical technology (PAT) compliance.\u003c\/p\u003e\n\u003ctable width=\"100%\" style=\"height: 758.6px;\"\u003e\n\u003ctbody\u003e\n\u003ctr style=\"height: 47.6px;\"\u003e\n\u003ctd style=\"width: 17.9856%; height: 47.6px;\"\u003e\u003cem\u003ePart Number\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd style=\"width: 81.6547%; height: 47.6px;\"\u003e\n\u003cul\u003e\n\u003cli\u003eEKMBABRMSS (EKM-BABR-MSS)\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr style=\"height: 67.2px;\"\u003e\n\u003ctd style=\"width: 17.9856%; height: 67.2px;\"\u003e\u003cem\u003ePower\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd style=\"width: 81.6547%; height: 67.2px;\"\u003e\n\u003cul\u003e\n\u003cli\u003eAC220V±10%, single phase, 50\/60Hz, ~2000 W \u003cbr\u003e\n\u003c\/li\u003e\n\u003cli\u003eA 3000 W converter can be used for AC110V condition\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr style=\"height: 380.8px;\"\u003e\n\u003ctd style=\"width: 17.9856%; height: 380.8px;\"\u003e\u003cem\u003eKey Features for Batch Reactor\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd style=\"width: 81.6547%; height: 380.8px;\"\u003e\n\u003cul\u003e\n\u003cli\u003eElectric-driven lifting module and equipped with pressure\/temperature thermocouple (MEAS\/OMEGA) and nickel-based alloy rapture disk\u003c\/li\u003e\n\u003cli\u003eFor standard 1L version, reactor cover is fixed and reactor vessel goes up\/down, while for 20-29 L, the reactor vessel is fixed and the reactor cover goes up\/down. \u003c\/li\u003e\n\u003cli\u003eAutomatic temperature loop: embedded with compressor for automatic cooling and heating cycling\u003c\/li\u003e\n\u003cli\u003eHMI touch screen for parameter setting and display, 30 programmable segments and RS485 communication port for computer connection. \u003cbr\u003e\n\u003c\/li\u003e\n\u003cli\u003eBatch Reactor Material: SS316L and Hastelloy C-276 (other material options, such as Ti alloy TA2, Zirconium 702, and Monel alloy 400 can be supplied upon request)\u003cbr\u003e\n\u003c\/li\u003e\n\u003cli\u003eReactor Volume: 1 L (standard benchtop version). Other large volume ground floor version, such as 2, 5, 10, 20, 29 L can be supplied upon request.\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003cp\u003e          \u003cimg style=\"float: none;\" alt=\"\" src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0774\/6591\/1526\/files\/EKMBABRMSS_04_100x100.jpg?v=1785023303\" width=\"94\" height=\"94\"\u003e      \u003cimg height=\"93\" width=\"93\" style=\"float: none;\" alt=\"\" src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0774\/6591\/1526\/files\/EKMBABRMSS_02_100x100.jpg?v=1785022973\"\u003e      \u003cimg style=\"float: none;\" alt=\"\" src=\"https:\/\/cdn.shopify.com\/s\/files\/1\/0774\/6591\/1526\/files\/EKMBABRMSS_03_100x100.jpg?v=1785023187\"\u003e    \u003c\/p\u003e\n\u003cul\u003e\n\u003cli\u003eOperation Temperature: -40°C ~ 300°C (2 kW), adjustable, over-temperature alarm, K-type thermocouple, heating rate of 3-5℃\/min\u003c\/li\u003e\n\u003cli\u003eHigh Pressure (standard version): Max. 10 MPa (WIKA vacuum gauge), overpressure alarm. A higher pressure of 20 MPa can be customized for 1L and 2L version.\u003cbr\u003e\n\u003c\/li\u003e\n\u003cli\u003eMechanical Shaft Stirring Speed: Max. 1200 rpm (1L). For other options, 1000 rpm (2L), 800 rpm (5L), 600 rpm (10 L), 300 rpm (20\/29 L)\u003c\/li\u003e\n\u003cli\u003eMechanical Shaft Stirring: propelled padel type (low viscosity fluid), high accuracy servo motor.\u003c\/li\u003e\n\u003cli\u003eHigh-quality Swagelok valves for gas inlet\/outlet. The safety valve (Fitok) is equipped for pressure relief. \u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr\u003e\n\u003ctd style=\"width: 17.9856%;\"\u003e\u003cem\u003eCustomizations (\u003cspan style=\"color: rgb(255, 42, 0);\"\u003eOptional\u003c\/span\u003e)\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd style=\"width: 81.6547%;\"\u003e\n\u003cul\u003e\n\u003cli\u003eSingle valve for sampling\u003c\/li\u003e\n\u003cli\u003eEquilibrium reflux sampling\u003c\/li\u003e\n\u003cli\u003eCooling Coil\u003cbr\u003e\n\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr style=\"height: 67.2px;\"\u003e\n\u003ctd style=\"width: 17.9856%; height: 67.2px;\"\u003e\u003cem\u003eCertification\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd style=\"width: 81.6547%; height: 67.2px;\"\u003e\n\u003cdiv style=\"text-align: left;\"\u003e\n\u003cul\u003e\n\u003cli\u003eCE certified\u003c\/li\u003e\n\u003cli\u003eUL and CSA certification is available upon request at extra cost\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/div\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr style=\"height: 47.6px;\"\u003e\n\u003ctd style=\"width: 17.9856%; height: 47.6px;\"\u003e\u003cem\u003eWarranty\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd style=\"width: 81.6547%; height: 47.6px;\"\u003e\n\u003cdiv style=\"text-align: left;\"\u003e\n\u003cul\u003e\n\u003cli\u003eOne year warranty and life-time technical support\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/div\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr style=\"height: 13.8px;\"\u003e\n\u003ctd style=\"width: 17.9856%; height: 13.8px;\"\u003e\u003cem\u003eDimension\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd style=\"width: 81.6547%; height: 13.8px;\"\u003e\n\u003cdiv style=\"text-align: left;\"\u003e\n\u003cul\u003e\n\u003cli\u003eL850*W590*H990mm (1L version)\u003cbr\u003e\n\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/div\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003ctr style=\"height: 47.6px;\"\u003e\n\u003ctd style=\"width: 17.9856%; height: 47.6px;\"\u003e\u003cem\u003eWeight\u003c\/em\u003e\u003c\/td\u003e\n\u003ctd style=\"width: 81.6547%; height: 47.6px;\"\u003e\n\u003cdiv style=\"text-align: left;\"\u003e\n\u003cul\u003e\n\u003cli\u003e~118 kg\u003c\/li\u003e\n\u003c\/ul\u003e\n\u003c\/div\u003e\n\u003c\/td\u003e\n\u003c\/tr\u003e\n\u003c\/tbody\u003e\n\u003c\/table\u003e\n\u003cp\u003e \u003c\/p\u003e\n\u003cp\u003e\u003cstrong\u003eReferences\u003c\/strong\u003e:\u003c\/p\u003e\n\u003col class=\"cus-ref-zone__list\"\u003e\n\u003cli\u003e\u003ca rel=\"noopener noreferrer\" href=\"https:\/\/www.sciencedirect.com\/science\/article\/abs\/pii\/S1385894712009060\" target=\"_blank\"\u003eN. Gemo, et al., Mass transfer and kinetics of H2O2 direct synthesis in a batch slurry reactor, Chemical Engineering Journal, 2012, 207, 539-551\u003c\/a\u003e\u003c\/li\u003e\n\u003cli\u003e\n\u003ca rel=\"noopener noreferrer\" href=\"https:\/\/www.nature.com\/articles\/s41467-022-31352-x\" target=\"_blank\"\u003eS. Yu, et al., Decoupled temperature and pressure hydrothermal synthesis of carbon sub-micron spheres from cellulose, Nature Communications, 2022, 13, 3616\u003c\/a\u003e.\u003c\/li\u003e\n\u003c\/ol\u003e","brand":"KMYQ","offers":[{"title":"SS316L","offer_id":48045059014886,"sku":"EKMBABRMSSS","price":17999.0,"currency_code":"USD","in_stock":true},{"title":"Hastelloy C276","offer_id":48045059047654,"sku":"EKMBABRMSSH","price":23999.0,"currency_code":"USD","in_stock":true}],"thumbnail_url":"\/\/cdn.shopify.com\/s\/files\/1\/0774\/6591\/1526\/files\/EKMBABRMSS_main.jpg?v=1785022518","url":"https:\/\/echemsupplies.com\/products\/ekmbabrmss","provider":"EChem Supplies","version":"1.0","type":"link"}