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SOFC/SOEC Planar Cell (5cm * 5cm or 10cm * 10cm) with Quartz Window for Operando Thermal Imaging Characterization, CSOFECOTICPCQW

SOFC/SOEC Planar Cell (5cm * 5cm or 10cm * 10cm) with Quartz Window for Operando Thermal Imaging Characterization, CSOFECOTICPCQW

In Stock SKU: CSOFECOTICPCQW55
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Advanced operando thermal imaging of planar SOFCs represents the frontier of electro-thermal characterization in the past few years. By integrating a quartz optical window into the test fixture, researchers can visualize real-time temperature gradients, hotspots, and redox dynamics that are otherwise invisible to standard thermocouples.

Designing a planar fixture with optical access requires balancing hermeticity (gas-tightness) with transparency. (1) Quartz Window Selection: Synthetic quartz or sapphire is used for its high transmissivity (>90%) in the 1.0 – 5.0 um range, which aligns with the mid-infrared (MWIR) cameras typically used for high-temperature thermography. (2) Window Placement: The window is usually integrated into the cathode manifold, allowing a direct line-of-sight to the electrode surface. This requires specialized high-temperature seals (e.g., gold gaskets or custom glass-ceramic) to prevent air from leaking into the fuel stream or cooling the cell surface prematurely. (3) Reflectivity & Emissivity: Since ceramics like LSM or LSC have high emissivity (~0.95-0.98), they are ideal for IR imaging. However, metallic components (interconnects) have low emissivity and can act as mirrors, reflecting the furnace elements. Proper emissivity correction is the most critical step in data post-processing.

Part Number
  • CSOFECOTICPCQW (C-SOFEC-OTIC-PCQW)
Test Fixture Features
  • The whole cell was made of alumina ceramic material without any risk of metal contamination
  • Ceramic spring compression part was designed for cell tightness.
  • Easy assemble/disassemble with electrode/electrolyte and conveniently placed inside the specific oven.
  • Complete accessories, such as current/voltage terminal, thermocouple terminal, and gas inlet/outlet ports. 
Main Specifications
  • Single Cell Size: 5cm * 5cm or 10cm * 10cm (square sheet)
  • Cell Fixture Size: W90 * D90 * H46 mm for 5cm*5cm cell

                                     W148 * D148 * H46 mm for 10cm* 10cm cell

  • Quartz Window: 40mm*40mm for 5cm*5cm cell

                                      80mm*80mm for 10cm*10cm cell

  • Max. Temperature: 900 °C
  • Gas Flow: Max. 2 L/min for 5cm*5cm; 3 L/min for 10cm*10cm
  • Gas Inlet/Outlet Port: φ 6 mm quick plug type
  • Pt/Ag Voltage Wire (φ 0.5mm/φ 1.5mm); Pt/Ag Current Wire (φ 0.5mm/φ 1.5mm); R-type thermocouple (φ 0.3mm). 
  • High Temperature Ceramic Sealant and Spring
Furnace & Temperature Control Integration (Optional)
  • The Furnace and temperature control can be integrated with the operando test cell (available upon request).

         

  • The inner size of furnace: W120 * D150 * H150 mm
  • The furnace external size: W280 * D310 * H340 mm
  • Observation Port was on the furnace side. 
  • Max. Temperature: 900 °C
  • Four-side heating mode
  • K-type thermocouple
Thermal Imaging Results
  • Anode: humidified 3% H2, 1000 mL/min; Cathode: 2000 mL/min (whole cell is under normal operation)

           

  • Anode: humidified 3% H2, 500 mL/min; Cathode: 1000 mL/min (S/C is too low, which cause cracks on the electrode surface during reforming reaction inside SOFC)

           

References:

  1. M. B. Pomfret, et al., Thermal imaging of solid oxide fuel cell anode processes, J. Power Source, 2010, 195, 257-262.
  2. D.J.L. Brett, et al., Application of infrared thermal imaging to the study of pellet solid oxide fuel cells, J. Power Sources, 2017, 258, 11, 1254-1261

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