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ECS-NM Molten Salt Electrolysis Furnace (Max. 1200℃), ENMMSEF

ECS-NM Molten Salt Electrolysis Furnace (Max. 1200℃), ENMMSEF

In Stock SKU: ENMMSEF
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A Molten Salt Electrolysis Furnace is a specialized high-temperature reactor designed for the electrochemical extraction of metals (like Li, Al, or Rare Earths) and the processing of advanced nuclear or solar thermal salts. It is a primary tool for studying the electrowinning of Lithium or the high-temperature behavior of halide/carbonate salts. The "Glovebox Compatible" requirement is critical because most molten salts (especially chlorides and fluorides) are highly hygroscopic and will react with moisture to form corrosive HCl or HF gases.

Unlike standard muffle furnaces, an molten salt electrolysis system must integrate high-current DC power with an ultra-dry, inert atmosphere to prevent the highly reactive molten metal from oxidizing or exploding upon contact with moisture. (1) Heating Zone: Modern industrial-grade units (like the ZYLAB G1200-600) utilize a combination of Bottom and Circumferential Ring Heating to ensure thermal uniformity. This prevents "cold spots" that can cause salt solidification and disrupt ion transport. (2) Reaction Chamber: Typically constructed from 316L Stainless Steel or Quartz with high-purity alumina fiber insulation. (3) DC Power Supply: High-current, low-voltage specifications are standard (e.g., 5V / 1000A). Precise current control is essential for managing the overpotential required to plate specific metals without triggering side reactions. (4) Electrode Setup: Often features a Titanium or Molybdenum cathode and a Graphite anode. In pilot systems, manual spiral feeders allow for semi-continuous operation without breaking the vacuum.

Part Number
  • ENMMSEF (ENM-MSEF)
Power
  • AC220V±10%, single phase, 50/60Hz, 9.5 kW 
General Features
  • High temperature stability and uniformity with resistance heating  
  • Dual-heating zones with individual temperature control
  • High purity alumina insulation layer for temperature maintenance.  
  • Anti-corrosion and sealing design: Al2O3, graphite, or special metal alloy-based heating hearth that is compatible with Cl-, F- corrosive molten salt. 
  • Inert gases (Ar/N2) could be flowed to maintain a O2/H2O-free environment
  • Electrochemical functions with reserved three-electrode ports; The high-temperature reference electrode (eg: Ag/AgCl, Bi/BiCl3) and conductive wires. 

           

Technical Features
  • Heating Temperature: Max. 1200℃ (accuracy: ±1℃) for short time (<30 min). Continuous operation at 1150℃
  • Thermocouple: K-type with φ2*280mm
  • Recommended Heating Rate: ≤10℃/min
  • Heating Hearth: Φ250*300mm
  • Al2O3 Crucible Sizes: (1) φ160*200mm (3L), 1 piece; (2) φ160*160mm (2.6L), 1 piece; (3) φ170*90mm (1.6L), 1 piece; (4) 310S crucible with φ168*233mm (5L), 2 pieces
  • Flow Meter: 0.1-1.5 L/min
  • Gas Inlet: Φ6.35mm double-clamps
  • Gas Outlet: D14 mm barber fitting
  • Vacuum Pump: DRV10 with KF25 connection port
  • Water Chiller Tank: 10 L 
Notes
  • Please do not open the furnace door when the temperature is higher than 300℃
  • The minor cracks on the furnace hearth during continuous operation is normal.
  • One-year warranty and life-time technical support & service 
Dimension
  • L880 * D760mm * H1150 mm
Weight
  • ~190 kg

 

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