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ECS-NM Vacuum Molten Salt Electrolysis Furnace (Max. 1200℃), ENMVMSEF

ECS-NM Vacuum Molten Salt Electrolysis Furnace (Max. 1200℃), ENMVMSEF

In Stock SKU: ENMVMSEF
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A Vacuum Molten Salt Electrolysis (VMSE) Furnace is a highly specialized reactor designed to perform electrolysis within a molten salt bath while maintaining a controlled vacuum or low-pressure environment.

While standard molten salt electrolysis furnaces operate under inert gas, a VMSE system provides three distinct advantages for high-purity battery research: (1) Enhanced Degassing: Vacuum pulls residual moisture and oxygen from the salt before melting, which is vital for Prussian Blue or NFPP synthesis where even trace H2O can cause lattice instability. (2) Low-Pressure Metal Collection: During the production of Metallic Sodium or Lithium, the vacuum helps in the "distillation" or separation of the metal from the electrolyte bath, leading to higher purity. (3) Removal of Halogen Gases: If you are electrolyzing chloride or fluoride salts, the vacuum system (paired with specialized scrubbers) ensures that toxic gases like Cl2 or F2 are efficiently removed from the reaction zone, protecting the heating elements from corrosion.

Part Number
  • ENMVMSEF (ENM-VMSEF)
Power
  • AC220V±10%, single phase, 50/60Hz, 8.8 kW 
General Features
  • Vacuum environment to avoid side reaction and get high purity electrolysis product
  • High temperature and uniform current distribution for flat and dense electroplating layer
  • Accurate temperature control system and fluctuation less than ±1℃.
  • Automatic molten salt feeding and discharge can be supplied upon request
  • Safety protection for over-heating and gas leaking alarm system.
Technical Features
  • Heating Temperature: Max. 1200℃ (accuracy: ±1℃) for short time (<30 min). Continuous operation at 1150℃
  • Thermocouple: K-type with φ2*280mm
  • Recommended Heating Rate: ≤10℃/min
  • Heating Hearth: Φ250*300mm, heating element: Mo-doped Fe-Cr-Al alloy
  • Reactor: 310S reactor with φ203*497mm (I.D. φ191 mm)

             

  • Al2O3 crucible with φ160*160mm (2650ml), 1 piece
  • Flow Meter: 0.1-1.5 L/min
  • Gas Inlet: Φ6.35mm double-clamps
  • Gas Outlet: D14 mm barber fitting
  • Vacuum Pump: DRV10 with KF25 connection port
  • Water Chiller Tank: 10 L 
Notes
  • Please do not open the furnace door when the temperature is higher than 300℃
  • The minor cracks on the furnace hearth during continuous operation is normal.
  • One-year warranty and life-time technical support & service 
Dimension
  • L880 * D760mm * H1150 mm
Weight
  • ~200 kg

 

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