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ECS-N Roll-to-Roll Three-Zones CVD Furnace (Max. 1200℃, 4" Quartz Tube) for 2D Material Synthesis, ENR2R3ZCVDF

ECS-N Roll-to-Roll Three-Zones CVD Furnace (Max. 1200℃, 4" Quartz Tube) for 2D Material Synthesis, ENR2R3ZCVDF

In Stock SKU: ENR2R3ZCVDF
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A Roll-to-Roll (R2R) CVD Furnace is the industrial gateway to mass-producing 2D materials like Graphene, Hexagonal Boron Nitride (h-BN), and Transition Metal Dichalcogenides (TMDs). Unlike batch furnaces, R2R systems continuously move a flexible substrate—typically copper or nickel foil—through a multi-zone heating chamber, allowing for the synthesis of 2D materials at meters-per-minute scales.

A professional R2R CVD platform consists of three integrated modules: (1) Unwinding Chamber: Holds the source roll (e.g., 25 um Copper foil). It features tension control to prevent the thin foil from wrinkling or tearing during high-temperature processing. (2) Multi-Zone Reaction Furnace: A long horizontal tube with multiple independent heating zones (1000℃ to 1200℃). This allows for a precise thermal profile: (a) Zone 1: Annealing/Pre-treatment (cleaning the foil surface). (b) Zone 2: Growth (introducing precursors like CH4 for graphene). (c) Zone 3: Controlled Cooling (crucial for maintaining crystal orientation). (3) Rewinding Chamber: Collects the finished material. In 2026 systems, this chamber is often vacuum-sealed or Ar-backfilled to prevent the freshly grown 2D layer from oxidizing.

Part Number
  • ENR2R3ZCVDF (EN-R2R3ZCVDF)
General Key Features
  • Continuous synthesis of 2D material with high efficiency
  • Support multiple vapor-deposition techniques and tandem processes integration
  • Various 2D materials, such as graphene, TMDs, hBN, MXene, can be synthesized with high flexibility
  • Different flexible substrates can be used for vapor deposition
  • HMI touch screen for easy setting and control 
R2R CVD Furnace System
  • AC380V±10%, three-phases, 50/60Hz, 10 kW
  • Maximum Heating Temperature: 1200℃ (<30 min)
  • Continuously Operation Temperature: ≤1100℃
  • Thermocouple: K-type (φ2*420mm)
  • Recommended Heating Rate: 10 ℃/min
  • Furnace Hearth: Φ150×800mm (three-zones, 200+400+200 mm)
  • Furnace Tube: Quartz, Φ100*1600*3mm
  • Four Channel Flow Meter: 1st-3rd channel: 1000 sccm; 4th channel: 3000 sccm; φ6.35 double clamp
  • Vacuum Pump: ≥4.4L/s, 13-12000 Pa, ultimate vacuum <5*10^(-2) torr. 
  • R2R Unit: Copper foil roll (2 kg, W80mm, T0.04 mm), web speed is 1-100 mm/min, adjustable
Notes
  • The door is not allowed to be opened when the furnace temperature higher than 300 ℃
  • The relative pressure inside the quart tube should less than 0.125 MPa 
  • Under high vacuum (10-3 torr) operation, the temperature should less than 800℃
  • The hazardous and flammable gases should be highly cautious, and the protections should be prepared before operation.
Certification
  • CE certified
  • UL and CSA certification is available upon request at extra cost
Dimension
  • L2700 × W900 × H1400 mm
Weight
  • ~530 kg

References:

V. D. Santo, et al., Tailored supported metal nanoparticles by CVD: an easy and efficient scale-up by a rotary bed OMCVD device, J. Mater. Chem., 2009,19, 9030-9037.

S. Tu, et al., Parametric investigation of in-situ synthesis of carbon nanotubes on Al2O3 powder by the rotary chemical vapor deposition method, Ceramics International, 2022, 48, 28258-28267 

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